Hydrochloric Acid → HCID 68121106, compound

HRID 1284194Notes

Reaction equation

HRID 1284194 reaction equation
[CH:1]1([C:4]([C:11]2[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][CH:12]=2)(O)[CH2:5][CH2:6][N:7]([CH3:9])[CH3:8])[CH2:3][CH2:2]1.[ClH:19]>CCOCC>[ClH:19].[Cl:19][CH2:3][CH2:2][CH:1]=[C:4]([C:11]1[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][CH:12]=1)[CH2:5][CH2:6][N:7]([CH3:9])[CH3:8]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19816157HCID 19816157, compound

Product 1

HCID 68121106HCID 68121106, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Procedure

1-Cyclopropyl-3-di-methylamino-1-(4-methoxyphenyl)- 1-propanol was dissolved in ether and ethereal hydrogen chloride was added to the ether solution. The ether insoluble hydrochloride salt was separated by filtration and recrystallized from isopropanol.

Workup

  1. customThe ether insoluble hydrochloride salt was separated by filtration
  2. customrecrystallized from isopropanol

Sources & evidence

ORD record
ord-dab83cfff787415c9502331241f44d93
Source dataset
uspto-grants-1976_08
Patent number
US03978129

Reaction notes

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