HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl formate → HCID 21515920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | 2-(alpha,alpha,beta,beta-Tetrafluorophenethyl)benzylamine | HCID 20372248 | — |
| Product | HCID 21515920 | HCID 21515920 | — |
Reaction Steps
2-(α,α,β,β-Tetrafluorophenethyl)benzylamine, 1.4 g. (0.005 mole), in 100 ml. of ethyl formate, is stirred and heated to refluxing for about 20 hours. Evaporation of the solution to dryness and trituration of the residual solid with petroleum ether gives N-[2-(α,α,β,β-tetrafluorophenethyl)benzyl]formamide, m.p. 61°-75°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03978127 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-45fe016111984fd9a917312ebb0d4386 |
| Source note | uspto-grants-1976_08 |