HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 12472499, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethylenethiourea | HCID 2723650 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12472499 | HCID 12472499 | — |
Reaction Steps
30.6 parts by weight of imidazolidine-2-thione were boiled overnight with 54.4 parts by weight of trimethylchlorosilane and 51.5 parts by weight of triethylamine in absolute tetrahydrofurane. The warm suspension was freed of the precipitated triethylamine hydrochloride by filtration, and the filtrate was evaporated and dried in a vacuum desiccator.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03978223 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-f69b391e25f540d7a1685f1175b1bffa |
| Source note | uspto-grants-1976_08 |