HuagongsheHuagongshe Chemistry Print Report · For research reference only
methyl P-methyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinate → P-methyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | methyl P-methyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinate | HCID 13564436 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | P-methyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinic acid | HCID 13564437 | — |
Reaction Steps
A solution of 1 g of methyl P-methyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinate in 10 ml of 6N HCl is refluxed for 16 hours. After cooling, the solid product is collected by filtration and dried, yielding P-methyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04563310 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-3e456314d3944a0dab0ef9560ee40e98 |
| Source note | uspto-grants-1986_01 |