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HRID1284418

反应详情

EQUATION

反应方程式

HRID 1284418 的结构方程式

REACTANTS

反应物

1
结构：COP(C)(=O)c1cc(Oc2ccc(C(F)(F)F)cc2Cl)ccc1[N+](=O)[O-]
HCID13564436

未命名化合物

PRODUCTS

生成物

1
结构：CP(=O)(O)c1cc(Oc2ccc(C(F)(F)F)cc2Cl)ccc1[N+](=O)[O-]
HCID13564437

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

PROCEDURE

实验过程

A solution of 1 g of methyl P-methyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinate in 10 ml of 6N HCl is refluxed for 16 hours. After cooling, the solid product is collected by filtration and dried, yielding P-methyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinic acid.

WORKUP

后处理

  1. temperatureAfter cooling
  2. filtrationthe solid product is collected by filtration
  3. customdried