Hydrochloric Acid → HCID 20454839, compound

HRID 1284423Notes

Reaction equation

[CH2:1]([P:4]([C:8]1[CH:13]=[C:12]([O:14][C:15]2[CH:20]=[CH:19][C:18]([C:21]([F:24])([F:23])[F:22])=[CH:17][C:16]=2[Cl:25])[CH:11]=[CH:10][C:9]=1[N+:26]([O-:28])=[O:27])(=[O:7])[O:5]C)[CH2:2][CH3:3].Cl>>[CH2:1]([P:4]([C:8]1[CH:13]=[C:12]([O:14][C:15]2[CH:20]=[CH:19][C:18]([C:21]([F:22])([F:24])[F:23])=[CH:17][C:16]=2[Cl:25])[CH:11]=[CH:10][C:9]=1[N+:26]([O-:28])=[O:27])(=[O:5])[OH:7])[CH2:2][CH3:3]

Participants

Reactant 2

HCID 313Hydrochloric Acid

HCID 54122799HCID 54122799, compound

Product 1

HCID 20454839HCID 20454839, compound

Procedure

Following the method of Example 3 or Example 13, methyl P-n-propyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinate and 6N HCl are reacted to give P-n-propyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinic acid.

Workup

customare reacted

Sources & evidence

ORD record: ord-9c0edf43c49745fc8134bb96c9b62dbd
Source dataset: uspto-grants-1986_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04563310

Reaction notes

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