HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 13423320, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | HCID 13417327 | HCID 13417327 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13423320 | HCID 13423320 | 91.6% |
Reaction Steps
(E)-7-Phenyl-7-(3-pyridyl)-6-hepten-1-ol (2.0 g, 7.4 mmoles) was reacted with methyl isocyanate (500 mg, 8.8 mmoles) in the presence of triethylamine in the same manner as Example 9 to give 1-methylaminocarbonyloxy-(E)-7-phenyl-7-(3-pyridyl)-6-heptene (2.2 g) (Compound Id-24) as an oil. This compound forms a crystalline salt of oxalic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04563446 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-09199850fa4e4dcf9f4355691ae2ec8a |
| Source note | uspto-grants-1986_01 |