HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl Isothiocyanate → HCID 13423327, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl Isothiocyanate | HCID 7673 | — |
| Reactant | HCID 13417327 | HCID 13417327 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13423327 | HCID 13423327 | — |
Reaction Steps
In the presence of triethylamine, (E)-7-phenyl-7-(3-pyridyl)-6-hepten-1-ol (2.0 g, 7.4 mmoles) was reacted with phenyl isothiocyanate (1.0 g, 7.5 mmoles) in the same manner as Example 9 to give 1-phenylaminothiocarbonyloxy-(E)-7-phenyl-7-(3-pyridyl)-6-heptene (Compound Id-28, 2.2 g) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04563446 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-6fcf2f84acc04b1ba19b731ef9c6ddc5 |
| Source note | uspto-grants-1986_01 |