HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 1H-Pyrrole, 3-nitro-1-(2,3,3-triiodo-2-propenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3-Nitropyrrole | HCID 145813 | — |
| Reactant | 2,3,3-Triiodoallyl-p-toluenesulfonate | HCID 13233003 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1H-Pyrrole, 3-nitro-1-(2,3,3-triiodo-2-propenyl)- | HCID 497088 | — |
Reaction Steps
To a solution of 112 mg (1 mmole) of 3-nitropyrrole in 5.0 ml of dry N,N-dimethylformamide were added 606 mg of 2,3,3-triiodoallyl-p-toluenesulfonate and 60 mg (1.5 mmoles) of powdery sodium hydroxide and the reaction was carried out with stirring for 15 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04563472 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-2686a8e13d744e82a4f34e52502c45de |
| Source note | uspto-grants-1986_01 |