HRID1284577

反应详情

EQUATION

反应方程式

HRID 1284577 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The powdered KOH is added slowly to the acrylic acid and the saccharose and water in a reaction flask kept in an ice-water bath. The temperature is kept between 40° and 50° C. After neutralization, the pH-value of the resulting solution is adjusted to 7.8. Then 2-hydroxyethyl methacrylate and the acetophenone are added. The mixture is then poured into the polymerization trough and polymerization is effected by UV-radiation at a bath temperature of 50° C. and a reaction temperature of 60° C. The product is readily millable.

WORKUP

后处理

  1. customis kept between 40° and 50° C
  2. additionThe mixture is then poured into the polymerization trough and polymerization
  3. customis effected by UV-radiation at a bath
  4. customtemperature of 50° C.
  5. customa reaction temperature of 60° C