HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoamyl Nitrite → HCID 54272265, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoamyl Nitrite | HCID 8053 | — |
| Reactant | HCID 53838271 | HCID 53838271 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54272265 | HCID 54272265 | — |
Reaction Steps
A suspension of 1 g of 8-amino-9-bromo-5H-pyrimido[5,4-b]indole-2-carboxylic acid ethyl ester in 70 ml of ethanol is combined with 1.8 ml of isoamyl nitrite. The mixture is refluxed for one hour and then concentrated. Yield: 0.2 g of 9-bromo-5H-pyrimido[5,4-b]indole-2-carboxylic acid ethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04564610 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-0235332ad24342a6b2dd71443305eff5 |
| Source note | uspto-grants-1986_01 |