HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20251303, compound → HCID 178448899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20251303 | HCID 20251303 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 178448899 | HCID 178448899 | — |
Reaction Steps
According to the method of Example 1, 3-butyramido-1-(3-trifluoromethylphenyl)-2-pyrazoline was reduced with lithium aluminium hydride to produce 3-butylamino-1-(3-trifluoromethylphenyl)-2-pyrazoline which was a gum (yield 2.4 g) and was recrystallized as the hydrochloride m.p. 173.4° (yield 1.65 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04564684 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-9ba3e0ccd45a4fe98ca21290e0eff78f |
| Source note | uspto-grants-1986_01 |