HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131714503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | HCID 20251344 | HCID 20251344 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 131714503 | HCID 131714503 | — |
Reaction Steps
9.86 g Of 2,3,7,8,9,9a-hexahydro-1H-phenalen-2-on was dissolved in 15 ml pyridine. A solution of 3.8 g hydroxylamine.HCl in 12 ml ethanol/H2O (1:1) was added to this solution and the mixture was stirred for one hour. The resultant deposit was filtered off, washed off H2O and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04564698 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-7386595377c54fe188ba0fd1b4c3be38 |
| Source note | uspto-grants-1986_01 |