Hydrochloric Acid → HCID 131714503, compound

HRID 1285014Notes

Reaction equation

HRID 1285014 reaction equation
[CH2:1]1[CH:12]2[C:13]3[C:4](=[CH:5][CH:6]=[CH:7][C:8]=3[CH2:9][CH2:10][CH2:11]2)[CH2:3][C:2]1=O.[NH2:15][OH:16].Cl>N1C=CC=CC=1.C(O)C.O>[CH2:1]1[CH:12]2[C:13]3[C:4](=[CH:5][CH:6]=[CH:7][C:8]=3[CH2:9][CH2:10][CH2:11]2)[CH2:3][C:2]1=[N:15][OH:16]

Participants

6

Reactant 3

HCID 313Hydrochloric AcidHCID 787HydroxylamineHCID 20251344HCID 20251344, compound

Product 1

HCID 131714503HCID 131714503, compound

Reagents, catalysts & solvents 2

HCID 1049PyridineSolventHCID 19096565Water ethanolSolvent

Procedure

9.86 g Of 2,3,7,8,9,9a-hexahydro-1H-phenalen-2-on was dissolved in 15 ml pyridine. A solution of 3.8 g hydroxylamine.HCl in 12 ml ethanol/H2O (1:1) was added to this solution and the mixture was stirred for one hour. The resultant deposit was filtered off, washed off H2O and dried.

Workup

  1. filtrationThe resultant deposit was filtered off
  2. washwashed off H2O
  3. customdried

Sources & evidence

ORD record
ord-7386595377c54fe188ba0fd1b4c3be38
Source dataset
uspto-grants-1986_01
Patent number
US04564698

Reaction notes

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