Hydrochloric Acid → HCID 20186257, compound

Participants

Reaction Steps

Next, 400 ml of (C2H5)2O was added to 6 g of Li[AlH4 ], and the resulting mixture was stirred. Thereto was very gradually added dropwise a (C2H5)2O solution including 36 g of the aforesaid methyl p-(4-pentylcyclohexyl)phenylacetate, and after completion of the addition, the thus obtained mixture was stirred at 30° C. or lower continuously for 3hours. The mixture was then poured into dilute hydrochloric acid and extracted with (C2H5)2O. After the (C2H5)2O was distilled off, the residue was recrystallized from n--C6H14 to obtain 4-[p-(2-hydroxyethyl)phenyl]pentylcyclohexane. The melting point of this compound was 44° to 46° C.

Provenance & Evidence