HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzyl Alcohol → Bromocresol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzyl Alcohol | HCID 125 | — |
| Reactant | Bromine | HCID 24408 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Bromocresol | HCID 41663 | — |
Reaction Steps
Dried bromine gas (Br2) was blown through a mixed solution of 33 g of p-hydroxybenzyl alcohol ##STR133## and 900 ml of benzene for 2 hours while cooling the solution with ice water. Thereafter, the solution was stirred for 2 hours, and then distilled to obtain p-hydroxybenzyl bromide ##STR134## The boiling point of this compound was 125°-126° C./15 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04564694 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-6704481c08674c2e803fa9170fb077b1 |
| Source note | uspto-grants-1986_01 |