HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-benzyloxy carbonyl-N-methyl-2-aminoethanol phosphocholine → 2-Methylaminoethanol phosphocholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-benzyloxy carbonyl-N-methyl-2-aminoethanol phosphocholine | HCID 86740600 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 2-Methylaminoethanol phosphocholine | HCID 86740599 | — |
Reaction Steps
8 g of N-benzyloxy carbonyl-N-methyl-2-aminoethanol phosphocholine are dissolved in 60 ml of dioxane and 15 ml of water; the solution is mixed with 0.8 g of 10% palladium active carbon and the reaction mixture hydrogenated with hydrogen. After the H2 -absorption has terminated, the solution is filtered and the filtrate reduced in vacuo to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04565659 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-a4844590bb254ef59569066638e47fec |
| Source note | uspto-grants-1986_01 |