Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 20249845 | HCID 20249845 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53661285 | HCID 53661285 | — |
Reaction Steps
9.7 ml of thionyl chloride was added dropwise with stirring to 34.4 g of 2-(4-t-hexyl-2-chlorophenoxy)capric acid dissolved in 34 ml of toluene heated to 60° C. The reaction was carried out at 60° C. for 2 hours. Excess thionyl chloride and toluene were distilled off under reduced pressure. 40.1 g of 2-(4-t-hexyl-2-chlorophenoxy)capric acid chloride was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04565777 |
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| Source dataset | uspto-grants-1986_01 |
|---|
| ORD ID | ord-5003b79af5d1431a8297f2013c08d450 |
|---|
| Source note | uspto-grants-1986_01 |
|---|
