HCID 20250470, compound → HCID 20250467, compound

Participants

Reaction Steps

3.97 g (12.7 mmole) of the compound from Example 33 was dissolved in 30 ml of methanol and 397 mg of 5% palladium on carbon was added. The resulting suspension was hydrogenated at 60 psi and 60° C. for 46 minutes. After cooling and removal of the catalyst by filtration, the solvent was removed by rotary evaporation to give 2.80 g (99%) of the title compound as a light yellow oil. Calc: C, 70.25; H, 8.16; Found: C, 69.54; H 8.18.

Provenance & Evidence