HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 2-[2-[[5-[(dimethylamino)methyl]furan-2-yl]methylsulfanyl]ethylamino]-3-methyl-4H-imidazol-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 5-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamine | HCID 162203 | — |
| Reactant | 1-Methyl-2-methylthio-imidazolin-4-one hydroiodide | HCID 20248950 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-[2-[[5-[(dimethylamino)methyl]furan-2-yl]methylsulfanyl]ethylamino]-3-methyl-4H-imidazol-5-one | HCID 178483219 | — |
Reaction Steps
2-(5-Dimethylaminomethylfuran-2-ylmethylthio)ethylamine (2.25 g), 1-methyl-2-methylthio-imidazolin-4-one hydroiodide (2.85 g) and triethylamine (3.635 g) were refluxed in ethanol (25 ml) for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04567176 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-e509d6c851424fabb3fce6a44bbf29d4 |
| Source note | uspto-grants-1986_01 |