Triethylamine → HCID 178483220, compound

HRID 1285331Notes

Reaction equation

HRID 1285331 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:9][C:8]([CH2:10][S:11][CH2:12][CH2:13][NH2:14])=[CH:7][CH:6]=1)[CH3:3].I.CS[C:18]1[NH:19][CH2:20][C:21](=[O:23])[N:22]=1.C(N(CC)CC)C>C(O)C>[CH3:3][N:2]([CH2:4][C:5]1[O:9][C:8]([CH2:10][S:11][CH2:12][CH2:13][NH:14][C:18]2[NH:19][CH2:20][C:21](=[O:23])[N:22]=2)=[CH:7][CH:6]=1)[CH3:1]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 1622035-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamineHCID 178503565HCID 178503565, compound

Product 1

HCID 178483220HCID 178483220, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

2-(5-Dimethylaminomethylfuran-2-ylmethylthio)ethylamine (4.00 g), 2-methylthio-imidazolin-4-one hydroiodide (9.63 g) and triethylamine (7.27 g) were refluxed in ethanol (50 ml) for 6 hours.

Sources & evidence

ORD record
ord-71f9507e917a46e4a51ff6361303180b
Source dataset
uspto-grants-1986_01
Patent number
US04567176

Reaction notes

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