HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromo(phenyl)acetic acid → HCID 91991162, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromo(phenyl)acetic acid | HCID 97919 | — |
| Reactant | HCID 178418395 | HCID 178418395 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 91991162 | HCID 91991162 | — |
Reaction Steps
A solution of 16.7 g (0.10 m) 2-mercaptobenzothiazole and 21.5 g (0.10 m) α-bromo-α-phenylacetic acid in acetone is heated to reflux for 5 hours and the solvent is then removed. The residual oil is triturated in acetone and 31 g of solid collected. The compound melts at 192°-4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04567267 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-2958e05113c546ea8ba3cc653dc4abec |
| Source note | uspto-grants-1986_01 |