HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aminoacetonitrile → HCID 13560802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aminoacetonitrile | HCID 10901 | — |
| Reactant | Chloro(phenyl)acetyl chloride | HCID 102902 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13560802 | HCID 13560802 | 80% |
Reaction Steps
9.2 g (0.10 m) aminoacetonitrile and 19.0 g (0.11 m) α-chlorophenylacetyl chloride are heated to reflux in methylene chloride for 4 hours. The reaction mixture is filtered and the solvent is removed. The residual solid is recrystallized from benzene to give 16.7 g (80% yield) of the title compound, which has a melting point of 73°-4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04567267 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-cf0c00d7fda142799e3eb96de83cf7e2 |
| Source note | uspto-grants-1986_01 |