HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 9860075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | BocGlyValOBzl | HCID 91977270 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 9860075 | HCID 9860075 | — |
Reaction Steps
To 9.0 g (20.6 mmoles) oily Boc-Gly-Val-OBzl (SEQ ID NO.14) were added 250 ml 2.6M HCl in EtOAc. The mixture was stirred for 80 min. and taken to dryness Under reduced pressure. Following repeated additions of EtoAc and evaporation to dryness under reduced pressure HCl, Gly-Val-OBzl (SEQ ID NO.9) was isolated as a white powder, Yield 5.6 g (79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05464821 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-3ae338f4064743da9bc1f73166759082 |
| Source note | uspto-grants-1995_11 |