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HRID128622

反应详情

EQUATION

反应方程式

HRID 128622 的结构方程式

REACTANTS

反应物

3
结构：O=[N+]([O-])c1ccc(Cl)cc1
HCID7474

1-Chloro-4-nitrobenzene

C6H4ClNO2

结构：O=C([O-])[O-].[Na+].[Na+]
HCID10340

Carbonic acid sodium salt (1:2)

CNa2O3

结构：O=[N+]([O-])c1ccc(OCCO)cc1
HCID85381

2-(4-Nitrophenoxy)ethanol

C8H9NO4

PRODUCTS

生成物

1
结构：Nc1ccc(OCCO)cc1
HCID80892

2-(4-Aminophenoxy)ethanol

C8H11NO2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：OCCO
溶剂HCID174

Ethylene glycol

C2H6O2

PROCEDURE

实验过程

2-(4-Aminophenoxy)ethanol was prepared, using the method described in Example C3, by the reduction of 2-(4-nitrophenoxy)ethanol which was prepared by heating a mixture of 4-chloronitrobenzene, ethylene glycol and sodium carbonate in a sealed vessel (Beil. 6, II, 222).

WORKUP

后处理

  1. customwas prepared
  2. temperatureby heating