HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylamine → HCID 4349298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | (1-Bromoethyl)benzene | HCID 11454 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 4349298 | HCID 4349298 | 95% |
Reaction Steps
Introduce 23 ml of propylamine into 200 ml of dimethylformamide, add 32 g of caesium carbonate and 9.25 g of α-methylbenzyl bromide. Leave for 4 hours at room temperature. Evaporate to dryness and take up with water. Extract with ethyl acetate, dry over anhydrous sodium sulphate and evaporate to dryness to obtain the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05464847 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-dfae9cc9acb94f7ca2a1b3598059a858 |
| Source note | uspto-grants-1995_11 |