HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → HCID 178496809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 178496819 | HCID 178496819 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178496809 | HCID 178496809 | 98.4% |
Reaction Steps
Following the procedure of Example IB, 7.2 g (0.05 mole) of the above isourea, 5.65 g (0.05 mole) of chloroacetyl chloride, 5.05 g (0.05 mole) of triethyl amine and 150 ml of tetrahydrofuran were combined to yield 11.6 g of N-morpholino-N'-(chloroacetyl)-O-methylisourea, nD30 1.4853.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984410 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-e8a7d192844f49f38924cabef37d216f |
| Source note | uspto-grants-1976_10 |