m-Chloroperbenzoic acid → HCID 131710465, compound

HRID 1287229Notes

Reaction equation

HRID 1287229 reaction equation
Cl.[C:2]([CH:10]1[C:15](=[O:16])[N:14]([CH2:17][CH2:18][CH2:19][N:20]([CH3:22])[CH3:21])[C:13]2[CH:23]=[CH:24][CH:25]=[CH:26][C:12]=2[S:11]1)(=[O:9])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[Cl:27]C1C=CC=C(C(OO)=[O:35])C=1>C(Cl)(Cl)Cl>[ClH:27].[C:2]([CH:10]1[C:15](=[O:16])[N:14]([CH2:17][CH2:18][CH2:19][N:20]([CH3:22])[CH3:21])[C:13]2[CH:23]=[CH:24][CH:25]=[CH:26][C:12]=2[S:11]1=[O:35])(=[O:9])[C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1

Participants

4

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 131710466HCID 131710466, compound

Product 1

HCID 131710465HCID 131710465, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

By treating the product from Example 2 (B) with a chloroform solution containing 1 equivalent of m-chloroperbenzoic acid and allowing the mixture to stand for about two hours at room temperature, the title product is obtained.

Sources & evidence

ORD record
ord-f5f9401cbddf48fc8574274f91a10376
Source dataset
uspto-grants-1976_10
Patent number
US03984405

Reaction notes

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