HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131710468, compound → HCID 131710467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131710468 | HCID 131710468 | — |
| Reactant | HCID 178418689 | HCID 178418689 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 131710467 | HCID 131710467 | — |
Reaction Steps
Interaction of the free base of the product of example 1 with 1 equivalent of CH3MgBr in ether at room temperature forms a Grignard complex which is decomposed with ice water and the ethereal solution dried over anhydrous MgSO4, filtered and the filtrate treated with anhydrous HCl to yield the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984405 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-ae71216fb25f4ab8a4c55764e0744bb1 |
| Source note | uspto-grants-1976_10 |