Hydrochloric Acid → HCID 131710472, compound

HRID 1287251Notes

Reaction equation

HRID 1287251 reaction equation
[CH3:1][C:2]([CH3:20])([NH2:19])[CH:3]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[CH2:11][CH2:12][N:13]1[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1)[NH2:4].[ClH:21]>CCOCC>[ClH:21].[ClH:21].[CH3:1][C:2]([CH3:20])([NH2:19])[CH:3]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[CH2:11][CH2:12][N:13]1[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1)[NH2:4]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21507575HCID 21507575, compound

Product 1

HCID 131710472HCID 131710472, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

To a solution of 1,1-dimethyl-2-[2-[2-(1-piperidinyl)ethyl]phenyl]-1,2-ethanediamine (2.7g) prepared as described in Example 3 in dry ether (50 ml) is added, with stirring and cooling, 10 ml of N ethereal hydrogen chloride solution, dropwise; the title compound separates out.

Workup

  1. additionis added
  2. temperaturecooling

Sources & evidence

ORD record
ord-bdec9b3547a2497296b361d454375083
Source dataset
uspto-grants-1976_10
Patent number
US03984421

Reaction notes

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