HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Lactate → HCID 53670576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Lactate | HCID 7344 | — |
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53670576 | HCID 53670576 | — |
Reaction Steps
The lactic acid ethyl ester and 1,4-dibromo-butane were reacted in THF in the presence of NaH to obtain 7-bromo-2-methyl-3-oxaheptanoic acid ethyl ester and subsequently, the exchange of bromine and iodine was carried out, as described in 4(d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984459 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-cdb7f651793b497ca7b1edb4335e92d8 |
| Source note | uspto-grants-1976_10 |