HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorophenyl isocyanate → HCID 152745232, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorophenyl isocyanate | HCID 76833 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Pentanimidamide Hydrochloride | HCID 11615174 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 152745232 | HCID 152745232 | — |
Reaction Steps
Following a procedure similar to that described in Example 1 but using 2.3 g. sodium in 250 ml. dry acetone, 13.6 g. valeramidine hydrochloride, and 15.3 g. 2-chlorophenyl isocyanate in 100 ml. dry acetone, there was obtained after recrystallization from isopropyl alcohol-ether 15.4 g. of the hydrochloride of 1-(2-chloropheyl)-3-(pentanimidoyl)yrea; m.p. 132°-134°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-8ac5c77aaca7416d863667685d42f5ae |
| Source note | uspto-grants-1976_10 |