HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorophenyl isocyanate → HCID 152745873, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorophenyl isocyanate | HCID 7607 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Pentanimidamide Hydrochloride | HCID 11615174 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 152745873 | HCID 152745873 | — |
Reaction Steps
Following a procedure similar to that described in Example 1 but using 3.39 g. sodium in 200 ml. dry acetone, 20 g. valeramidine hydrochloride, and 27.6 g. 3,4-dichlorophenyl isocyanate in 100 ml. dry acetone, there was obtained after recrystallization from acetone 10.5 g. of the hydrochloride of 1-(3,4-dichlorophenyl)-3-(pentanimidoyl)urea; m.p. 177°-179°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-a597ad27cdbd44cabb8c86e73ea5e928 |
| Source note | uspto-grants-1976_10 |