HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-isocyanato-4-nitro- → HCID 152747114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-isocyanato-4-nitro- | HCID 66012 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Pentanimidamide Hydrochloride | HCID 11615174 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 152747114 | HCID 152747114 | — |
Reaction Steps
Following a procedure similar to that described in Example 1 but using 3.39 g. sodium in 200 ml. dry acetone, 20 g. valeramidine hydrochloride, and 21.9 g. 4-nitrophenyl isocyanate in 100 ml. dry acetone, there was obtained after recrystallization from methyl alcohol 10.8 g. of the hydrochloride of 1-(4-nitrophenyl)-3(-pentanimidoyl)urea; m.p. 187°-191°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-85618ed00bf94c3caefa7e7aa06939d6 |
| Source note | uspto-grants-1976_10 |