HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-chloro-3-isocyanato- → HCID 152746173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-chloro-3-isocyanato- | HCID 17968 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Pentanimidamide Hydrochloride | HCID 11615174 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 152746173 | HCID 152746173 | — |
Reaction Steps
Following a procedure similar to that described in Example 1 but using 6.9 g. sodium in 300 ml. dry acetone, 41.1 g. valeramidine hydrochloride, and 46.2 g. 3-chlorophenyl isocyanate in 200 ml. dry acetone, there was obtained after recrystallization from acetone 27.1 g. of tjhe hydrochloride of 1-(3-chlorophenyl)-3-(pentanimidoyl)urea; m.p. 135°-137°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-0c9b241bc4b94459adef2d4707295fe3 |
| Source note | uspto-grants-1976_10 |