HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 152745163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Pentanimidamide Hydrochloride | HCID 11615174 | — |
| Reactant | 1-(Benzyloxy)-2-isocyanatobenzene | HCID 18373464 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 152745163 | HCID 152745163 | — |
Reaction Steps
Following a procedure similar to that described in Example 1 but using 2.9 g. sodium in 300 ml. dry acetone, 17.7 g. valeramidine hydrochloride, and 29.3 g. 2-(benzyloxy)phenyl isocyanate in 200 ml. dry acetone, there was obtained after recrystallization from isopropyl alcohol 33.9 g. of the hydrochloride of 1-[2-(benzyloxy)phenyl]-3-(pentanimidoyl)urea; m.p. 145°-147°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-afca6e9f54dc42189e391d4362bcb184 |
| Source note | uspto-grants-1976_10 |