HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 152750107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Pentanimidamide Hydrochloride | HCID 11615174 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 152750107 | HCID 152750107 | — |
Reaction Steps
Following a procedure similar to that described in Example 23 but using 6.9 g. sodium in 300 ml. dry acetone, 41.1 g. valeramidine hydrochloride, and 35.7 g. phenyl isocyanate in 200 ml. dry acetone, there was obtained after recrystallization from ethyl alcohol 40.3 g. 1-phenyl-3-(pentanimidoyl)urea hydrochloride; m.p. 155.5°-156°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-8cc68c00677f44e08aead840e0a18f54 |
| Source note | uspto-grants-1976_10 |