HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 152750100, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | Acetamidine monohydrochloride | HCID 67170 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 152750100 | HCID 152750100 | — |
Reaction Steps
Following a procedure similar to that described in Example 23 but using 4.6 g. sodium in 500 ml. dry acetone, 18.8 g. acetamidine hydrochloride and 23.8 g. phenyl isocyanate in 100 ml. dry acetone, there was obtained after recrystallization from isopropyl alcohol 27.1 g. 1-phenyl-3-(acetimidoyl)urea hydrochloride; m.p. 204°-206°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-a0d8a2bb3f4d4497a764216f47ebddf7 |
| Source note | uspto-grants-1976_10 |