HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl isocyanate → HCID 152748181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl isocyanate | HCID 8110 | — |
| Reactant | Benzamidine, hydrochloride | HCID 80289 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 152748181 | HCID 152748181 | — |
Reaction Steps
Following a procedure similar to that described in Example 23 but using 7.7 g. sodium in 1100 ml. dry sodium, 52.4 g. benzamidine hydrochloride, and 33.1 g. butylisocyanate in 400 ml. dry acetone there was obtained, after recrystallization from ethyl acetate, 62.2 g. 1-butyl-3-(benzimidoyl)urea hydrochloride; m.p. 139°-141°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-4cf6b54dfb5d4e788e781efd6f02028a |
| Source note | uspto-grants-1976_10 |