Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → HCID 178444019, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | 1,2-Dichloro-4-isothiocyanatobenzene | HCID 23065 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 반응물 | Heptanimidamide hydrochloride | HCID 14144282 | — |
| 용매 | Benzene n-pentane | HCID 19707280 | — |
| 생성물 | HCID 178444019 | HCID 178444019 | — |
반응 단계
Following a procedure similar to that described in Example 42 but using 2.3 g. sodium in 250 ml. dry acetone, 16.4 g. heptanamidine hydrochloride, and 20.4 g. 3,4-dichlorophenyl isothiocyanate (b.p. 149-152/15-16 mm.) in 150 ml. dry acetone there was obtained 1-(3,4-dichlorophenyl)-3-(heptanimidoyl)-2-thiourea, m.p. 89°-90°C. (from benzene-n-pentane); hydrochloride (27 g.), m.p. 158°-160°C. (from acetonitrile).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03984467 |
| 출처 데이터셋 | uspto-grants-1976_10 |
| ORD ID | ord-a52a41c90bf44443947889596549e339 |
| 출처 메모 | uspto-grants-1976_10 |