HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 178443512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 4-Chlorophenyl isothiocyanate | HCID 16480 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 20095019 | HCID 20095019 | — |
| Solvent | Benzene hexane | HCID 110624 | — |
| Product | HCID 178443512 | HCID 178443512 | — |
Reaction Steps
Following a procedure similar to that described in Example 42 but using 1.9 g. sodium in 200 ml. dry acetone, 16 g. nonanamidine hydrochloride, and 14.2 g. 4-chlorophenyl isothiocyanate in 100 ml. dry acetone there was obtained 1-(4-chlorophenyl)-3-(nonanimidoyl)-2-thiourea, m.p. 102°-103°C. (from benzene-n-hexane); hydrochloride (16.2 g.); m.p. 172°-174°C. (from acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-4ae5f7d5f08a40be8bc6284fde572b10 |
| Source note | uspto-grants-1976_10 |