HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenyl isothiocyanate → HCID 178444018, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenyl isothiocyanate | HCID 16480 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 21508134 | HCID 21508134 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178444018 | HCID 178444018 | — |
Reaction Steps
Following a procedure similar to that described in Example 42 but using 3.8 g. sodium in 350 ml. dry acetone, 27.2 g. 3-ethylvaleramidine hydrochloride, and 27 g. 4-chlorophenyl isothiocyanate in 175 ml. dry acetone there was obtained 1-(4-chlorophenyl)-3-(3-ethylpentanimidoyl)-2-thiourea; m.p. 116°-118°C. (from acetonitrile); hydrochloride (42.7 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-c578eb97ae2145a5a9a4251e69f734c1 |
| Source note | uspto-grants-1976_10 |