HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenyl isothiocyanate → HCID 178483422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenyl isothiocyanate | HCID 16480 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 21508022 | HCID 21508022 | — |
| Reactant | HCID 178483423 | HCID 178483423 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 178483422 | HCID 178483422 | — |
Reaction Steps
Following a procedure similar to that described in Example 42 but using 2.8 g. sodium in 300 ml. dry acetone, 18.5 g. 11-(dimethylamino)undecanamidine dihydrochloride, and 11.9 g. 4-chlorophenyl isothiocyanate in 100 ml. dry acetone there was obtained 10.4 g. 1-(4-chlorophenyl)-3-[11-(dimethylamino)undecanimidoyl]-2-thiourea dihydrochloride; m.p. 130°-132°C. (from isopropyl alcohol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-f72f554cb4b74c33b655fdb1c1ff6301 |
| Source note | uspto-grants-1976_10 |