HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenyl Isocyanate → HCID 152746817, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenyl Isocyanate | HCID 7693 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 131710477 | HCID 131710477 | — |
| Reactant | HCID 178483448 | HCID 178483448 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 152746817 | HCID 152746817 | — |
Reaction Steps
Following a procedure similar to that described in Example 33A but using 1.7 g. sodium in 300 ml. dry acetone, 9 g. 5-(dimethylamino)valeramidine dihydrochloride hemihydrate [m.p. 119°-120°C. (from acetonitrile)], and 5.8 g. 4-chlorophenyl isocyanate in 50 ml. dry acetone there was obtained 8.5 g. 1-(4-chlorophenyl)-3-[5-(dimethylamino)pentanimidoyl]urea dihydrochloride; m.p. 199°-200°C. (from isopropyl alcohol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-93cc4ec43bd54c38b91e7bd6059ed655 |
| Source note | uspto-grants-1976_10 |