HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl (ethoxymethylene)malonate → HCID 21508898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl (ethoxymethylene)malonate | HCID 6871 | — |
| Reactant | HCID 21508901 | HCID 21508901 | — |
| Product | HCID 21508898 | HCID 21508898 | — |
Reaction Steps
Using the method of Example 1 diethyl ethoxymethylene malonate is reacted with 3,4-dihydro-6-methoxy-3-methyl-2H-1,4-benzoxazine and the product reacted with polyphosphoric acid to provide ethyl 2,3-dihydro-8-methoxy-3-methyl-7-oxo-7H-pyrido[1,2,3-de]-1,4-benzoxazine-6-carboxylate, m.p. 165°-168° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984548 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-71f4a37569974de5b962a1830613876d |
| Source note | uspto-grants-1976_10 |