HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichloroanisole → HCID 12395646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichloroanisole | HCID 16126 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 7-bromoheptanoyl Chloride | HCID 11368152 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 12395646 | HCID 12395646 | — |
Reaction Steps
The title compound is prepared following substantially the same procedure described in Example 13, Step A, using the following substances: 2,3-dichloroanisole (89 g., 0.5 mole), 7-bromoheptanoyl chloride (127 g., 0.56 mole), aluminum chloride (74 g., 0.56 mole) and methylene chloride (500 ml.). This procedure affords 107 g. (58%) of 2,3-dichloro-4-(7-bromoheptanoyl)anisole which after recrystallization from the cyclohexane melts at 57°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984465 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-f42600f44d95444db5d2312bdc255ead |
| Source note | uspto-grants-1976_10 |