Hydrochloric Acid → HCID 21509166, compound

HRID 1287505Notes

Reaction equation

HRID 1287505 reaction equation
Cl.[NH:2]=[C:3]1[C:11]([CH3:13])([CH3:12])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]1[CH3:14].[Cl:15][C:16]1[CH:24]=[CH:23][C:19]([C:20](Cl)=[O:21])=[CH:18][CH:17]=1>N1C=CC=CC=1>[Cl:15][C:16]1[CH:24]=[CH:23][C:19]([C:20]([N:2]=[C:3]2[C:11]([CH3:12])([CH3:13])[C:10]3[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=3)[N:4]2[CH3:14])=[O:21])=[CH:18][CH:17]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 85014-Chlorobenzoyl chlorideHCID 4283796HCID 4283796, compound

Product 1

HCID 21509166HCID 21509166, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

By reacting 15 g. of the hydrochloride of 2-imino-1,3,3-trimethylindoline (m.p. 271°-273° C) in 100 ml. of pyridine with 16.30 g. of p-chlorobenzoylchloride at the room temperature for 5 hours, 15.2 g. of the title compound are obtained. B.p. 192° C/0.1 mmHg.

Sources & evidence

ORD record
ord-56dd96d3ad1a4ae69e489be5e2bdee0d
Source dataset
uspto-grants-1976_10
Patent number
US03984563

Reaction notes

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