Hydrochloric Acid → HCID 131710489, compound

HRID 1287649Notes

Reaction equation

HRID 1287649 reaction equation
[CH3:1][NH:2][C:3]1[C:4]2[C:17]([CH3:18])=[N:16][O:15][C:5]=2[N:6]=[C:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:8]=1.[ClH:19]>C(#N)C>[ClH:19].[CH3:1][NH:2][C:3]1[C:4]2[C:17]([CH3:18])=[N:16][O:15][C:5]=2[N:6]=[C:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:8]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21505699N,3-Dimethyl-6-phenyl[1,2]oxazolo[5,4-b]pyridin-4-amine

Product 1

HCID 131710489HCID 131710489, compoundYield 88.3%

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

The hydrochloride is prepared by dissolving N, 3-dimethyl-6-phenylisoxazolo[5,4-b]pyridin-4-amine in acetonitrile and adding ethereal hydrochloric acid, yield 88.3%, m.p. 232°-234°.

Sources & evidence

ORD record
ord-b85d210d6b334664a2841cbbf9e00f4d
Source dataset
uspto-grants-1976_10
Patent number
US03985760

Reaction notes

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