Diethylamine → HCID 21903177, compound

Participants

Reaction Steps

Anhydrous diethylamine (0.11 moles) is added dropwise to a stirred solution of α-chloro-β-(3-chloro-4-cyclohexylphenyl)propionic acid (0.10 moles) in 100 ml. of n-hexane at 0°C. The precipitate is collected on a filter, washed with n-hexane, and dried in a vacuum desiccator to obtain α-chloro-β-(3-chloro-4-cyclohexylphenyl(propionic acid, diethylammonium salt.

Provenance & Evidence