Diethylamine → HCID 21903177, compound

HRID 1287679Notes

Reaction equation

HRID 1287679 reaction equation
[CH2:1]([NH:3][CH2:4][CH3:5])[CH3:2].Cl[CH:7]([CH2:11]C1C=CC(C2CCCCC2)=C(Cl)C=1)[C:8]([OH:10])=[O:9]>CCCCCC>[CH2:1]([NH2+:3][CH2:4][CH3:5])[CH3:2].[C:8]([O-:10])(=[O:9])[CH2:7][CH3:11]

Participants

4

Reactant 2

HCID 8021DiethylamineHCID 21506230HCID 21506230, compound

Product 1

HCID 21903177HCID 21903177, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Anhydrous diethylamine (0.11 moles) is added dropwise to a stirred solution of α-chloro-β-(3-chloro-4-cyclohexylphenyl)propionic acid (0.10 moles) in 100 ml. of n-hexane at 0°C. The precipitate is collected on a filter, washed with n-hexane, and dried in a vacuum desiccator to obtain α-chloro-β-(3-chloro-4-cyclohexylphenyl(propionic acid, diethylammonium salt.

Workup

  1. customat 0°C
  2. customThe precipitate is collected on a filter
  3. washwashed with n-hexane
  4. customdried in a vacuum desiccator

Sources & evidence

ORD record
ord-f1a25af7bddd4e8fa1edd56c146cd487
Source dataset
uspto-grants-1976_10
Patent number
US03985788

Reaction notes

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